基础化学实验:中英对照版

第一篇 基础化学实验基本知识第一章 实验室规则及安全知识 1．基础化学实验目的 2．化学实验室一般规则 3．化学实验室的安全知识 4．化学实验操作过程中可能发生的事故与处理 5．化学实验室的防火、防电与灭火常识第二章 基础化学实验常用仪器 1．实验室常用仪器介绍 2．玻璃仪器的洗涤和干燥 3．常用仪器使用方法第三章 实验结果的表示 1．实验误差与有效数字 2．实验数据的处理 3．实验报告第二篇 基础化学实验课题 实验课题一 基本操作训练实验 实验一 常用容量分析仪器操作练习 实验二 电子天平称量练习 实验三 缓冲溶液的配制与性质、溶液pH测定 实验四 胶体溶液的制备与性质 实验课题二 滴定分析实验 实验五酸碱滴定分析法 1．标准盐酸溶液浓度的标定 2．标准氢氧化钠溶液浓度的标定 3．食用醋中总酸度的测定 4．硼砂含量的测定 5．返滴定法测定阿司匹林的含量 实验六 氧化还原滴定法 1．高锰酸钾法 2．碘量法 实验七 配位滴定分析 1．水的硬度的测定 2．明矾含量的测定 3．葡萄糖酸钙含量的测定 实验课题三 分光光度法实验 实验八 可见分光光度法测定水样中铁含量 1．邻二 氮菲法 2．硫氰酸盐法 3．磺基水杨酸法 实验九 分光光度法测定阿司匹林药片的含量 实验十 分光光度法测定磺基水杨酸合铁的组成和稳定常数 实验十一 荧光分析法测定维生素B2的含量 实验十二 紫外分光光度法对维生素B12的鉴别与含量测定 实验课题四 化学原理实验 实验十三 稀溶液的依数性及其应用 1．凝固点降低法测定溶质的分子量 2．利用溶液的渗透浓度测定溶质的相对分子质量 3．冰点渗透压计的应用 实验十四 置换法测定镁的原子量 实验十五 化学反应速率与活化能的测定 实验十六 最大气泡压力法测定乙醇溶液的表面张力 实验课题五 化合物制备实验 实验十七 氯化钠的精制 实验十八 硫酸亚铁铵的制备 实验十九 转化法制备硝酸钾 实验课题六 综合及研究性实验 实验二十 醋酸解离常数的测定与食醋中HAc含量的测定 实验二十一 茶叶中钙、镁及铁含量的测定 实验课题七 自行设计实验 实验二十二 实验设计及研究 Part Ⅰ Experiment Essentials in Basic Chemistry Chapter l Laboratory Rules and Safety Information 1. The Purpose of Experiments in Basic Chemistry 2. General Rules in Laboratory 3. Safety Information 4. The Treatment of Accidents in Chemical Experiments 5. Fire Prevention, Anti-electricity and Extinguishing Knowledge Chapter 2 Ordinary Instruments in Chemical Experiments 1. Introduction of Ordinary Instruments in Chemical Laboratory 2. Cleaning and Drying Glasswares 3. Operation of Instrument Chapter 3 Experiment Results and their Expressions 1. Experimental Error and Significant Figures 2. Treatments of Experimental Data 3. Experiment Reports Part Ⅱ Experiments in Basic Chemistry Chapter 1 Experiments of Basic Operation Practice Experiment 1 Operation of Volumetric Analysis Experiment 2 Weighing Practice with an Electronic Balance Experiment 3 Preparation, Properties and pH Measurement of Buffer Solutions Experiment 4 Preparation and Properties of Colloidal Systems Chapter 2 Experiments of Titration Analysis Experiment 5 Acid-Base Titration Analysis 1. Standardization of the Concentration of HCI Solution 2. Standardization of the Concentration of NaOH Solution 3. Determination of Acetic Acid Content in Vinegar 4. Determination of Borax Content 5. Determination of Aspirin Content by Back Titration Experiment 6 Oxidation-Reduction Titration 1. Potassium Permanganate Method 2. lodimetry Experiment 7 Complexometric Titration 1. Determination of Water Hardness 2. Determination of KAl(SO4)2·12H2O in Alum 3. Determination of Calcium Gluconate Chapter 3 Spectrophotometry Experiment 8 Determination of Fe3+ (Fe2+) Content in Water Sample with Visible Spectrophotometry 1. O-phenanthroline Method 2. Sulfocyanate Method 3. Sulfosalicylic Acid Method Experiment 9 Determination of Aspirin Content in Tablets by Visible Spectrophotometry Experiment 10 Determination of the Formula and the Stability Constant of Sulfosalicylate Iron (Ⅲ) by Spectrophotometry Experiment 11 Determination of Vitamin B2 by Fluorescence Analysis Experiment 12 Identification and Content Determination of Vitamin B12 by Ultraviolet Spectrophotometry Chapter 4 Chemical Principles Experiment Experiment 13 Colligative Properties of Dilute Solution and Their Application 1. Determination of Molar Mass of Glucose by Freezing Point Depression 2. Determination of the Molar Mass of Glucose by Determining Osmolarity 3. Application of Freezing Point Osmometer Experiment 14 Determination of the Relative Atomic Mass of Magnesium by Replacement Reaction Experiment 15 Determination of the Rate of Chemical Reaction and Activation Energy Experiment 16 The Maximum Bubble Pressure Method to Determine the Surface Tension of Ethanol Solution Chapter 5 Preparation of Compounds Experiment 17 Refining Sodium Chloride Experiment 18 Preparation of Ammonium Iron (U) Sulfate Experiment 19 Preparation of Potassium Nitrate by Conversion Method Chapter 6 Comprehensive Experiments Experiment 20 Determination of HAc Content and Dissociation Equilibrium Constant of Content of HAc Experiment 21 Determination of the Content of Calcium, Magnesium, and Iron in Tea Chapter 7 Self-Designed Experiment Experiment 22 Design and Research附录 附录Ⅰ 国际相对原子量表 附录Ⅱ 不同温度下水的饱和蒸汽压 附录Ⅲ 危险药品的分类、性质和管理 附录Ⅳ 标准缓冲溶液 附录Ⅴ 参考书目